Preparation of Experiments on Growing Zinc–Cadmium Telluride Crystals in Microgravity

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Дәйексөз келтіру

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Аннотация

Cd1-xZnxTe crystals are necessary for the production of ionizing radiation detectors widely used in science, technology, medicine and other fields. Internal stresses during crystallization lead to generation of dislocations and low-angle boundaries. Typical problem of melt crystal growth of Cd-Zn-Te compounds are tellurium inclusions, which deteriorate detector performance. Microgravity conditions provide unique opportunities for growing high-quality crystals due to the absence of convection, more equilibrium conditions of melt mixing, and a decrease in internal stresses. Since the properties of such crystals strongly depend on the production conditions, seeds and a feed ingot with specified compositions and structure are required. Ampoules with two compositions of materials have been prepared for the space experiment. Crystals of different compositions Cd0.96Zn0.04Te and Cd0.9Zn0.1Te were produced for two charges. They consist of an oriented seed, solvent, and feeding ingot, which are single-phased, single crystalline, have certain crystallographic orientation, meet demands for growth of Cd–Zn–Te crystals in microgravity. Ampoules containing these materials were sent to International Space Station for crystal growth on equipment already assembled at “Nauka” station.

Толық мәтін

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Авторлар туралы

А. Аzhgalieva

Osipyan Institute of Solid State Physics of the RAS

Хат алмасуға жауапты Автор.
Email: azhgalieva@issp.ac.ru
Ресей, Chernogolovka

Е. Borisenko

Osipyan Institute of Solid State Physics of the RAS

Email: borisenk@issp.ac.ru
Ресей, Chernogolovka

D. Borisenko

Osipyan Institute of Solid State Physics of the RAS

Email: azhgalieva@issp.ac.ru
Ресей, Chernogolovka

А. Burmistrov

Research and Development Institute for Launch Complexes

Email: azhgalieva@issp.ac.ru
Ресей, Moscow

N. Кolesnikov

Osipyan Institute of Solid State Physics of the RAS

Email: azhgalieva@issp.ac.ru
Ресей, Chernogolovka

А. Тimonina

Osipyan Institute of Solid State Physics of the RAS

Email: azhgalieva@issp.ac.ru
Ресей, Chernogolovka

А. Senchenkov

Research and Development Institute for Launch Complexes

Email: azhgalieva@issp.ac.ru
Ресей, Moscow

Т. Fursova

Osipyan Institute of Solid State Physics of the RAS

Email: azhgalieva@issp.ac.ru
Ресей, Chernogolovka

О. Shakhlevich

Osipyan Institute of Solid State Physics of the RAS

Email: azhgalieva@issp.ac.ru
Ресей, Chernogolovka

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2. Fig. 1. Lauegram of the sample of composition Cd0.96Zn0.04Te

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3. Fig. 2. Ampoule for crystal growth in microgravity: a) - assembly drawing: 1 - ampoule, 2 - inoculum, 3 - solvent zone, 4 - feed ingot, 5 - insert, 6 - spring, 7 - filler, 8 - stopper; b) - general view with loading after assembly and hermetic sealing

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4. Fig. 3. Results of X-ray phase analysis of the sample of composition Cd0.96Zn0.04Te

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5. Fig. 4. Axial distribution of components of Cd0.9Zn0.1Te crystal according to X-ray spectral analysis data

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6. Fig. 5. Transmission spectra of the samples of composition Cd0.9Zn0.1Te (a) and Cd0.96Zn0.04Te (b) in the visible range: a sharp change in transmittance occurs at the emission wavelengths of 790 and 817 nm, respectively

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